PARSTAT 3000A-DX Bipotentiostat/Galvanostat

The PARSTAT 3000A-DX from Princeton Applied Research is both a hardware synchronized bipotentiostat/galvanostat and dual channel potentiostat/galvanostat in one.  The compact design, based on the popular PARSTAT 3000A, combines 2 high performance, independent potentiostats in a single chassis.  Combine this with a hardware synchronized start and the VersaStudio software platform for a fully functional bipotentiostat that is suitable for a range of applications from mechanistic studies and electrocatalyst evaluation using a rotating ring disk electrode (RRDE) to sensor development.

Key features of the PARSTAT 3000A-DX include:

  • +/- 2 A of current and +/- 30 V polarization and compliance
  • Up to 7 MHz EIS as standard
  • 4 nA (120 fA resolution) as standard
  • 6-WIRE capability to measure an auxiliary voltage
  • Floating ground
  • Data acquisition rate of up to 1000 kS/sec (1 µs time per point) 

As a true bipotentiostat the PARSTAT 3000A-DX can control the signal and measure the response of two different working electrodes in the same cell with separate or shared reference and counter electrodes.  The floating capability and hardware synchronization of the PARSTAT 3000A-DX, along with the wide range of available techniques in VersaStudio, make for an ideal and flexible bipotentiostat/galvanostat.  Princeton Applied Research also offers rotators, RRDE electrodes and associated accessories for a complete RRDE setup.

When not used as a bipotentiostat, the PARSTAT 3000A-DX can run two asynchronous experiments on completely separate electrochemical cells.  The outstanding specifications accommodate a range of applications highlighted below.

  • +/- 30 V compliance – Corrosion analysis in low conductivity electrolyte, large surface area samples and non-aqueous electrochemistry, including ionic liquids and molten salts
  • +/-30 V polarization – Study of high voltage batteries and battery stacks 
  • Wide dynamic current range (+/- 2 A to 4 nA) – 10 current ranges allow for detection of a low concentration analyte common in electroanalytical chemistry and measurement of high currents associated with high surface area nanostructured electrodes for capacitor development
  • 7 MHz EIS – Solid-state materials analysis and measurements of equivalent series resistance (ESR) and uncompensated resistance
  • 6-WIRE – Simultaneous DC and EIS measurements of anode/cathode or single cell/complete stack
  • Documents +

  • Specifications +


    PARSTAT 3000A-DX Channel 1 PARSTAT 3000A-DX Channel 2
    Data Acquisition
    Data Acquisition 3 x 16 bit 500 k samples per second ADCs Synchronized voltage/current/auxiliary 4 x 18 bit 1000 k samples per second ADCs Synchronized voltage/current/auxiliary/6-WIRE
    Time Base Resolution 2 µs (500 k samples/second) 1 µs (1000 k samples/second)
    Automatic Noise Filters Enabled/disabled Enabled/disabled
    Power Amplifier
    Voltage Compliance ±12 V ±30 V
    Current Compliance ±2 A ±1 A
    Potentiostat Bandwidth 1 MHz 7 MHz
    Stability Settings Auto and User Selectable Auto and User Selectable
    Rise Time          
    (-1.0V to +1.0V)
    < 500 ns (typical)
    56 ns (typical)
    Voltage Control (Potentiostat Mode)
    Applied Voltage Range ±10 V ±6 V, ±30 V 
    Applied Voltage Resolution for ±10 mV signal = 305 nV
    for ±100 mV signal = 3 µV
    for ±1 V signal = 30 µV
    for ±10 V signal = 300 µV
    for ±10 mV signal = 305 nV
    for ±100 mV signal = 3 µV
    for ±1 V signal = 30 µV
    for ±6 V signal = 183 µV
    Applied Voltage Accuracy ±0.2% of value ±2 mV ±0.2% of value ±2 mV
    Maximum Scan Rate for a 25 mV step = 12,500 Vs-1 for a 25 mV step = 25,000 Vs-1
    Current Control (Galvanostatic Mode)
    Applied Current  0 to ±2 A 0 to ±1 A
    Applied Current Accuracy ±0.2% of reading, ±0.2% of range ±200 pA ±0.2% of reading, ±0.2% of range ±200 pA
    Maximum Resolution 62 µA 62 µA
    Minimum Resolution 6.1 pA 6.1 pA
    Electrometer
    Maximum Input Range ±10 V ±30 V
    Bandwidth ≥10 MHz (-3 dB) ≥10 MHz (-3 dB)
    Input Impedance ≥1012 Ω in parallel with ≤5 pF (typical) ≥1013 Ω in parallel with ≤5 pF (typical)
    Leakage Current ≤5 pA at less than 25°C ≤5 pA at less than 25°C
    CMRR ≥60 dB at 100 kHz (typical) ≥70 dB at 300 kHz, ≥55 db at 100 kHz (typical)
    Voltage Measurement
    Voltage Range ±10 V ±6 V, ±30 V 
    Minimum Resolution 6 µV 915 nV, 5 µV 
    Voltage Accuracy ±0.2% of reading, ±2 mV ±0.2% of reading, ±2 mV
    Current Measurement
    Current Ranges Auto-ranging (10 ranges) 2 A to 4 nA Auto-ranging (10 ranges) 1 A to 4 nA
    Current Resolution 122 fA 31 fA
    Current Accuracy (DC) 20 nA to 2 A: ±0.2% of reading, ±0.2% of range
    4 nA: <0.5% ±20 pA
    20 nA to 1 A: ±0.2% of reading, ±0.2% of range
    4 nA: ±0.2% of reading, ±0.2% of range ±50 pA
    Bandwidth ≥1 MHz for ≥2 mA range (typical) ≥5 MHz for ≥2 mA range (typical)
    Bandwidth limit filter Yes Yes
    Impedance (EIS) Available with P3KA-DX CH1 and CH2
    Mode Potentiostat/Galvanostatic Potentiostat/Galvanostatic
    Frequency Ranges 1 MHz to 10 µHz  7 MHz to 10 µHz 
    Minimum AC Voltage Amplitude 0.1 mV RMS 0.1 mV RMS
    Sweep Linear or Logarithmic Linear or Logarithmic
    iR Compensation
    Positive Feedback Yes Yes
    Dynamic iR Yes Yes
    Interfaces (Optional BNC Cables)
    Signal Monitors E and I E1, E2 and I
    Digital inputs/outputs 5 TTL logic outputs, 2 TTL logic inputs 5 TTL logic outputs, 2 TTL logic inputs
    SYNC ADC
    Auxiliary Voltage Input
    Measurement synchronized to V and I ±10 V range, input impedance 10 kΩ
    9 pin connector standard
    Measurement synchronized to V and I ±10 V range, input impedance 10 kΩ (scaled 6:1)
    9 pin connector standard
    DAC Voltage Output (Standard) ±10 V range, output impedance 1 kΩ
    9 pin connector standard (for stirrers, rotating disk electrode etc.)
    ±10 V range, output impedance 1 kΩ
    9 pin connector standard (for stirrers, rotating disk electrode etc.)
    PC/Software
    Communications Interface Universal Serial Bus (USB) Universal Serial Bus (USB)
    Operating System Windows 10/8/7 (64-bit & 32-bit), Windows XP Windows 10/8/7 (64-bit & 32-bit), Windows XP
    PC Specification (recommended) Intel Core i5 or equivalent / 4 GB memory, High Data rates may require additional memory Intel Core i5 or equivalent / 4 GB memory, High Data rates may require additional memory
    Software VersaStudio, VersaStudio Developer's Kit (VDK) VersaStudio, VersaStudio Developer's Kit (VDK)
    General
    Ground (Selectable) Isolated (floating) / Earth Isolated (floating) / Earth
    Dimensions 25.1 cm x 9.5 cm x 40.1 cm 25.1 cm x 9.5 cm x 40.1 cm
    Operating Temperature Range 10°C to 35°C 10°C to 35°C
    Humidity Maximum 80% non-condensing Maximum 80% non-condensing
    Temperature (specified) 25°C 25°C
    Dummy Cell Internal (1 per channel) and external (1 per chassis) Internal (1 per channel) and external (1 per chassis)
    CE Approved Yes Yes

    ±1A
    ±1A
    ±1A
    0 to ±2A
    ≥10 
    ≥10 
  • Accessories +

    • LC Low Current Interface

      • Designed as a plug-in add on to extend the low current capability of many of the Princeton Applied Research potentiostats

      • Femtoampere accuracy and attoampere resolution for both DC and AC (EIS) measurements

      • Auto-current ranging capability from 200 mA - 4 pA (80 fA minimum range with PARSTAT 4000A)

      • 5 selectable E and I filters for noise reduction

      Keep Reading

    • 636A RRDE Rotating Ring-Disk Electrode

      Rotating Ring-Disk Electrode

      • Disk or Ring-Disk configuration
      • Protective enclosure
      • Remote analog speed control (input is summed with front-panel settings)
      • A variety of disk and ring-disk electrodes to choose from
      • Interchangeable electrode assemblies in either disk or cylinder configurations for corrosion studies
      • On/off and Rotational Rate Control

      Keep Reading

    • 616A Rotating Disk Electrode

      Rotating Disk Electrode

      • Front-panel speed controls
      • Protective enclosure
      • Remote analog speed control (input is summed with front-panel settings)
      • Front-panel and remote (TTL) on/off switching
      • Remote analog output for speed verification
      • Integral ring-stand for convenient cell mounting

      Keep Reading

    • QCM922A Quartz Crystal Microbalance and EQCM

      Quartz Crystal Microbalance

      • Sensitive enough to measure weight changes in a monolayer 
      • Quantify both elastic and viscous changes in your system
      • Front panel display of resonant frequency and resistance changes
      • Frequency range of 1MHz to 10MHz
      • Designed for EQCM with a potentiostat or stand alone operation

      Keep Reading

    • Battery Holders

      • Replaces the standard cell cable by connecting directly to the potentiostat
      • 5 options are available for the following form factors:  18650, AA, AAA, coin cell (2032) and a flexible screw-based design for custom cell geometries

      Keep Reading

    • K0235 Flat Cell Kit

      • Optimal construction for corrosion/coatings studies of flat specimens having a range of sizes and geometry

      • Specially designed gasket to minimize crevice corrosion

      • Platinum mesh counter electrode and Ag/AgCl reference electrode included

      • Exposed sample area is 1 cm2 with an option for a larger exposed area of 12.6 cm2

      Keep Reading

    • K0047 Corrosion Cell Kit

      • Ideal for corrosion analysis of cylindrical metal specimens with an optional sample holder to accommodate flat specimens

      • Cell configuration is modeled after a design commonly found in many ASTM standards

      • Supplied with graphite counter electrodes and saturated calomel reference electrode (SCE)

      • Jacketed version is available for studies at elevated temperatures

      Keep Reading

    • RDE0018 Analytical Cell Kit

      • Designed with two cell top configurations, one for general use and the other for accommodating a rotating electrode (RDE, RRDE, RCE) connected to the 616 or 636 A/B rotator

      • Supplied with a platinum wire counter electrode and Ag/AgCl reference electrode

      • Standard 14/20 tapper joints can accommodate a variety of working electrodes and reference electrode chemistries

      • Operates with solution volumes from 5 – 50 mL

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    • K0264 Micro-Cell Kit

      • Intended to be used for any application where solution volume is limited, requiring volumes ranging from 3 to 15 mL

      • Purge tube assembly provided for bubbling or blanketing the solution with inert gas

      • Platinum wire counter electrode and Ag/AgCl reference electrode included

      • Compatible with a range of working electrode materials available in two sizes: 2 mm or 10 µm diameter

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    • K0307 Tait Cell Kit

      • Designed specifically for corrosion studies on flat specimens under conditions where typical reference electrodes are incompatible

      • Hastelloy C-276 reference and counter electrodes included

      • Exposed sample area of 32 cm2

      • Holds volumes as low as 80 mL

      Keep Reading

    • Faraday Cage

      • Designed to shield anything housed in the cage from the effects of external electric fields, thereby reducing noise from interfering with the experiment
      • Standard faraday cage is 27 x 30 x 41 cm and is large enough to accommodate the VersaSTAT LC
      • An oversized faraday cage designed for use with the VersaSCAN is also available

      Keep Reading

  • Video +

    Watch video demonstrations of the PARSTAT 3000A-DX Bipotentiostat/Galvanostat

  • Software +

    • VersaStudio Software

      • Functional software platform used to control various Princeton Applied Research potentiostats/galvanostats (VersaSTAT and PARSTAT series) with the option of sequencing potentiostatic, galvanostatic and impedance capabilities for versatile experiment design.

      • Simple to use, straight forward data comparison and convenient data analysis and fitting routines, such as Tafel, polarization resistance and peak analysis.  Text file format allows easy importing of data into other graphing software for further analysis and/or report generation.

      • New versions made easily accessible with free download from our website without the need for registration.  Collaborators and coworkers, without access to an instrument, can also install the software for manageable data sharing. 

      Keep Reading

    • ZSimpWin

      • High performing electrochemical impedance spectroscopy (EIS) data analysis software that easily interfaces with the VersaStudio software platform.
      • Minimal user input without the need for the starting values and simple, single-click fitting procedures.
      • Various options from pre-loaded circuit models to user created and saved models.  Output results using a range of plot formats and easily view estimated parameters and historical records of computation process.

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